(AsPh4)2[Re3Cl„(H2O)]·H2O, previously thought to be (AsPh4)2[Re3Cl11], was redetermined from single-crystal four-circle diffractometer data. The crystal system is triclinic, PĪ, a = 983.1(6), b = 1200.5(6), c = 2566.2(10) pm, α = 92.67(4), β = 99.95(4), γ = 113.38(2)°, Vm = 817.95(1) cm3/mol, R = 0.043,Rw= 0.033.
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