Darstellung und Kristallstruktur von [H3N(CH2)3NH3]SbCl5

du Bois, André; Abriel, Walter

dc.identifier.uri	http://dx.doi.org/10.15488/2467
dc.identifier.uri	http://www.repo.uni-hannover.de/handle/123456789/2493
dc.contributor.author	du Bois, André
dc.contributor.author	Abriel, Walter
dc.date.accessioned	2017-11-24T11:46:32Z
dc.date.available	2017-11-24T11:46:32Z
dc.date.issued	1989
dc.identifier.citation	du Bois, A.; Abriel, W.: Darstellung und Kristallstruktur von [H3N(CH2)3NH3]SbCl5. In: Zeitschrift für Naturforschung - Section B Journal of Chemical Sciences 44 (1989), Nr. 9, S. 1151-1154. DOI: https://doi.org/10.1515/znb-1989-0925
dc.description.abstract	Using 293 K diffractometer intensity data, the structure of [H3N(CH2)3NH3]SbCl5 has been determined by single crystal X-ray technique and refined to a final Rw of 0.026. The colorless crystals are monoclinic (space group P21/c) with a = 10.1338(5), b = 11.4623(7), c = 11.3668(6) Å, β = 113.52(5)° and Ζ = 4. The structure contains ψ-octahedral SbCl52- anions. A center of symmetry connects two anions forming a (Sb2Cl10)4- unit with rather long Sb—Cl distances for the bridging Cl-atoms (2.92 and 3.68 A, respectively).	eng
dc.language.iso	ger
dc.publisher	Berlin : De Gruyter
dc.relation.ispartofseries	Zeitschrift für Naturforschung - Section B Journal of Chemical Sciences 44 (1989), Nr. 9
dc.rights	CC BY-NC-ND 3.0 Unported
dc.rights.uri	https://creativecommons.org/licenses/by-nc-nd/3.0/
dc.subject	Antimonates	eng
dc.subject	Crystal Structure	eng
dc.subject	Lone Pair Electrons	eng
dc.subject.ddc	540 \| Chemie	ger
dc.title	Darstellung und Kristallstruktur von [H3N(CH2)3NH3]SbCl5	ger
dc.type	Article
dc.type	Text
dc.relation.essn	1865-7117
dc.relation.issn	0932-0776
dc.relation.doi	https://doi.org/10.1515/znb-1989-0925
dc.bibliographicCitation.issue	9
dc.bibliographicCitation.volume	44
dc.bibliographicCitation.firstPage	1151
dc.bibliographicCitation.lastPage	1154
dc.description.version	publishedVersion
tib.accessRights	frei zug�nglich