Darstellung und Kristallstruktur von [H3N(CH2)3NH3]SbCl5

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dc.identifier.uri http://dx.doi.org/10.15488/2467
dc.identifier.uri http://www.repo.uni-hannover.de/handle/123456789/2493
dc.contributor.author du Bois, André
dc.contributor.author Abriel, Walter
dc.date.accessioned 2017-11-24T11:46:32Z
dc.date.available 2017-11-24T11:46:32Z
dc.date.issued 1989
dc.identifier.citation du Bois, A.; Abriel, W.: Darstellung und Kristallstruktur von [H3N(CH2)3NH3]SbCl5. In: Zeitschrift für Naturforschung - Section B Journal of Chemical Sciences 44 (1989), Nr. 9, S. 1151-1154. DOI: https://doi.org/10.1515/znb-1989-0925
dc.description.abstract Using 293 K diffractometer intensity data, the structure of [H3N(CH2)3NH3]SbCl5 has been determined by single crystal X-ray technique and refined to a final Rw of 0.026. The colorless crystals are monoclinic (space group P21/c) with a = 10.1338(5), b = 11.4623(7), c = 11.3668(6) Å, β = 113.52(5)° and Ζ = 4. The structure contains ψ-octahedral SbCl52- anions. A center of symmetry connects two anions forming a (Sb2Cl10)4- unit with rather long Sb—Cl distances for the bridging Cl-atoms (2.92 and 3.68 A, respectively). eng
dc.language.iso ger
dc.publisher Berlin : De Gruyter
dc.relation.ispartofseries Zeitschrift für Naturforschung - Section B Journal of Chemical Sciences 44 (1989), Nr. 9
dc.rights CC BY-NC-ND 3.0 Unported
dc.rights.uri https://creativecommons.org/licenses/by-nc-nd/3.0/
dc.subject Antimonates eng
dc.subject Crystal Structure eng
dc.subject Lone Pair Electrons eng
dc.subject.ddc 540 | Chemie ger
dc.title Darstellung und Kristallstruktur von [H3N(CH2)3NH3]SbCl5 ger
dc.type article
dc.type Text
dc.relation.essn 1865-7117
dc.relation.issn 0932-0776
dc.relation.doi https://doi.org/10.1515/znb-1989-0925
dc.bibliographicCitation.issue 9
dc.bibliographicCitation.volume 44
dc.bibliographicCitation.firstPage 1151
dc.bibliographicCitation.lastPage 1154
dc.description.version publishedVersion
tib.accessRights frei zug�nglich

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