Browsing by Subject "crystallisation"

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Formate modulated solvothermal synthesis of ZIF-8 investigated using time-resolved in situ X-ray diffraction and scanning electron microscopy

Cravillon, Janosch; Schröder, Christian A.; Bux, Helge; Rothkirch, André; Caro, Jürgen; Wiebcke, Michael (Cambridge : Royal Society of Chemistry, 2012)

Time-resolved investigations using in situ energy-dispersive X-ray diffraction in tandem with ex situscanning electron microscopy revealed that solvothermal crystallisation of ZIF-8 in methanol solvent and in the presence ...
Subtle polymorphism of zinc imidazolate frameworks: Temperature-dependent ground states in the energy landscape revealed by experiment and theory

Schröder, Christian A.; Baburin, Igor A.; van Wüllen, Leo; Wiebcke, Michael; Leoni, Stefano (Cambridge : Royal Society of Chemistry, 2013)

We show by variable-temperature X-ray diffraction and differential scanning calorimetry experiments that zinc imidazolates with coi and zni framework topology, respectively represent the thermodynamically stable phase below ...

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